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EnglishThe heat capacity calibration constants of a commercial MTDSC instrument were determined in a variety of experimental conditions. For a given modulation frequency, the calibration constants are the same within a few percents for different temperatures and over a wide range of scan rates and modulation amplitudes. On the other hand, the modulation constants change substantially with the period. Rules to optimize the accuracy of the system are given.
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http://hdl.handle.net/11571/2493| Titolo: | MTDSC Calibration: dependence of the instrumental response upon experimental conditions. |
| Autori interni: | MARINI, AMEDEO BERBENNI, VITTORIO BRUNI, GIOVANNA |
| Data di pubblicazione: | 1999 |
| Rivista: | JOURNAL OF THERMAL ANALYSIS |
| Abstract: | The heat capacity calibration constants of a commercial MTDSC instrument were determined in a variety of experimental conditions. For a given modulation frequency, the calibration constants are the same within a few percents for different temperatures and over a wide range of scan rates and modulation amplitudes. On the other hand, the modulation constants change substantially with the period. Rules to optimize the accuracy of the system are given. |
| Handle: | http://hdl.handle.net/11571/2493 |
| Appare nelle tipologie: | 1.1 Articolo in rivista |
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